Glycol mediated synthesis of Green Rust, its Delamination and Solvothermal Decomposition of the resulting colloidal dispersion to form monodispersed γ-Fe2O3 Nanoparticles

Jyothi Sequeira

doi:10.36948/ijfmr.2026.v08i01.67593

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Glycol mediated synthesis of Green Rust, its Delamination and Solvothermal Decomposition of the resulting colloidal dispersion to form monodispersed γ-Fe2O3 Nanoparticles

Author(s)	Dr. Jyothi Sequeira
Country	India
Abstract	Hydroxychloride green rust was synthesized by urea hydrolysis of ferric chloride in ethylene glycol. The chloride ions of green rust were then exchanged with the surfactant anion, dodecylsulphate (DS). Surfactant-intercalated green rust (GRDS) delaminated in 1,2-propanediol to give a stable colloidal dispersion of monolayers. Solvothermal decomposition of the colloidal dispersion resulted in monodispersed, single crystalline meghamite, γ-Fe2O3 nanoparticles of ~10 nm diameter.
Keywords	Hydroxychloride green rust, delamination, γ-Fe2O3 nanoparticles
Field	Chemistry
Published In	Volume 8, Issue 1, January-February 2026
Published On	2026-01-30
DOI	https://doi.org/10.36948/ijfmr.2026.v08i01.67593

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Glycol mediated synthesis of Green Rust, its Delamination and Solvothermal Decomposition of the resulting colloidal dispersion to form monodispersed γ-Fe2O3 Nanoparticles

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